A system and method for distillation testing of a liquid sample at atmospheric pressure for the improved prediction of the heating necessary to reach the initial boiling point (IBP) and ensure the IBP is observed within certain time constraints, and regardless of sample composition. This monitors the sample by the camera during different heating phases of the test to obtain visual images of the sample and a computer analyzes image data observed to regulate the optimal distillation process.

Cryogenic device analysis systems are provided that can include: a cold source within a first vacuum chamber; a cryogenic device mount within a second vacuum chamber, wherein the first and second vacuum chambers are separated by a vacuum barrier; a first thermal conduit extending from the cold source through the vacuum barrier to the sample mount; a first thermal switch along the first thermal conduit and operatively aligned between the cold source and the vacuum barrier. Methods for performing analysis of a cryogenic device are also provided.

Cryogenic device analysis systems are provided that can include: a cold source within a first vacuum chamber; a cryogenic device mount within a second vacuum chamber, wherein the first and second vacuum chambers are separated by a vacuum barrier; a first thermal conduit extending from the cold source through the vacuum barrier to the sample mount; a first thermal switch along the first thermal conduit and operatively aligned between the cold source and the vacuum barrier. Methods for performing analysis of a cryogenic device are also provided.

A distillation head with fraction collector is disclosed. In embodiments thereof, the fraction collector has a bottom portal which is raised up from the floor or bottom thereof. Fractions which condense fall to the floor and a lip of the bottom portal, raised from the floor of the fraction collector, prevents condensed fractions from falling downwards through a path of entry. Rather, condensed fractions exit in liquid form out a side portal. The fraction collector further has side walls which are, in embodiments, partially vertical and/or partially curvilinear and/or partially bulbous. The distillation head also can have a top portal through which a vacuum can be applied.

An apparatus and a process for testing fluid from a heat exchanger. A first fluid from a heat exchanger to be tested is passed through a test heat exchanger. A second, heat transfer fluid, is in the test heat exchanger. The second fluid is heated with a heater so that a temperature in the test heat exchanger can be controlled, for example, to so that conditions in the heat exchanger are close to the conditions in the heat exchanger. After a period of time, the test heat exchanger can be removed and inspected, tested, or both. Also, multiple test heat exchangers may be used to test various process conditions. Additionally, the test heat exchangers may include different materials to test various materials. An outer portion of the test heat exchanger may be at least semi-transparent.

A distillation head with fraction collector is disclosed. In embodiments thereof, the fraction collector has a bottom portal which is raised up from the floor or bottom thereof. Fractions which condense fall to the floor and a lip of the bottom portal, raised from the floor of the fraction collector, prevents condensed fractions from falling downwards through a path of entry. Rather, condensed fractions exit in liquid form out a side portal. The fraction collector further has side walls which are, in embodiments, partially vertical and/or partially curvilinear and/or partially bulbous. The distillation head also can have a top portal through which a vacuum can be applied.

Examples relate to cryogen flow control techniques using a magnetic failsafe valve. The valve is located between a cryogen source and a cryogen bath and has a position based on the magnetic field generated by a parallel solenoid circuit having a superconducting solenoid wound in a first direction and a non-superconducting solenoid (e.g., normal metal solenoid) wound in a second direction. When the current source is supplying a current to the parallel solenoid circuit and the temperature at the parallel solenoid circuit is below a threshold temperature, the current flows through the superconducting solenoid causing the magnetic field generated by the parallel solenoid circuit to position the magnetic valve in a particular state (e.g., open). The position of the valve can quickly change in situations where the temperature rises above the threshold temperature.

Switch assemblies for a cryogenic device analysis system are provided. The switch assembly can include: a cold source conductive member extending lengthwise to a cold source; and a cryogenic device conductive member extending lengthwise to a cryogenic device and at least partially overlapping at least a portion of the cold source conductive member. Methods for closing a conductive connection between a cold source and a cryogenic device within a cryogenic analysis system are provided. Methods for opening a conductive connection between a cold source and a cryogenic device within a cryogenic analysis system are provided. Cryogenic device analysis systems are also provided.

An apparatus and a process for testing fluid from a heat exchanger. A first fluid from a heat exchanger to be tested is passed through a test heat exchanger. A second, heat transfer fluid, is in the test heat exchanger. The second fluid is heated with a heater so that a temperature in the test heat exchanger can be controlled, for example, to so that conditions in the heat exchanger are close to the conditions in the heat exchanger. After a period of time, the test heat exchanger can be removed and inspected, tested, or both. Also, multiple test heat exchangers may be used to test various process conditions. Additionally, the test heat exchangers may include different materials to test various materials. An outer portion of the test heat exchanger may be at least semi-transparent.

The invention relates to a method and device for measuring the dew point of humid gases, and more particularly to determining the humidity of gas mixtures according to the dew point, and can be used in all fields in which measurements of this sort are required. The claimed device is capable of determining a dew point in a range of from +45 C. to +95 C., which corresponds to a moisture content of from 65 to 3000 g of water per 1 kg of dry air. The device performs continuous measurement. The essence of the invention is that the claimed method for measuring dew point consists in determining the point of a sudden change in the temperature gradient along a tubular cooler through which the humid gas under examination is passed, and calculating the temperature at which this change takes place. The tubular cooler is cooled by the surrounding air. The device has a generator for generating an output signal that transmits information about the parameters of the gas to external systems and that can be used as an input signal for a moisture content regulator. The device can be equipped with a digital indicator for displaying the gas parameters obtained.