B01J2219/00236

SYSTEMS AND METHODS FOR PREDICTING AND CONTROLLING THE PROPERTIES OF A CHEMICAL SPECIES DURING A TIME-DEPENDENT PROCESS
20180011024 · 2018-01-11 ·

Devices and methods for controlling the properties of chemical species during time-dependent processes. A device includes a reactor for containing one or more chemical species of a time-dependent process, an extraction pump for automatically and continuously extracting an amount of the one or more chemical species from the reactor, one or more detectors for measuring property changes of the one or more extracted chemical species and generating a continuous stream of data related to the one or more property changes to the one or more chemical species during a time interval, and a process controller configured to fit the continuous stream of data to a mathematical function to predict one or more properties of the one or more chemical species at a future time point and make one or more process decisions based on the prediction of one or more properties at the future time point.

Overpressure protection in hot high pressure processing systems in multi-stage up-flow reactor systems
11549072 · 2023-01-10 · ·

The invention relates to an improved system and method for relief of hot, high pressure, fouling fluid from the 1.sup.st Stage Reactor and the ISS in case of an unintended overpressure situation while allowing the quick establishing of normal fluid flow path once the overpressure situation has been corrected. This allows for rapid cooling of all subsequent reactor stages while minimizing VGO slop generation that needs reprocessing.

Actuator with port

An actuator is provided that includes a housing, a linear actuating shaft disposed within the housing, a piston coupled with the shaft, and a fluid barrier disposed on an end of the shaft and encircled by the piston. The piston is movable longitudinally between an extended configuration and a retracted configuration upon rotation of the shaft. The fluid barrier engages an inner surface of the piston preventing fluid communication across the fluid barrier. The fluid barrier has a shaft engaging side which receives the shaft and a fluid facing side. A cavity is formed between the piston and the fluid facing side and expands when the piston moves to the extended configuration and contracts when the piston moves to the retracted configuration. A port is disposed in the piston and extends from the cavity to external the piston thereby permitting fluid communication between the cavity and external the piston.

BED LEVEL SENSOR FOR SOLID BEDS WITH LEVELING ACTUATORS

A biochar production system includes a reactor body, a central rod disposed within the reactor body, a leveling arm extending from the central rod and configured to rotate about the central rod, and a bed level sensor system. The bed level sensor system includes a float configured to move from a resting position on a biomass in the reactor to an ending position upon contact with the leveling arm, and a level sensor coupled to the float via a connector. The level sensor is configured to correspondingly move with the float. A controller is configured to detect bed levels of the biomass within the reactor body, and determine a plurality of sample readings based on the detected bed levels.

Multi-compartment reactor and method for controlling retention time in a multi-compartment reactor

A method is disclosed for controlling retention time in a reactor, such as an autoclave, having a plurality of compartments separated by dividers with underflow openings. A retention time of the reaction mixture is calculated and compared with an optimal retention time, and the volumes of the reaction mixture in the compartments are adjusted while maintaining the flow rate of the reaction mixture, so as to change the retention time to a value which is closer to the optimal retention time. The reactor may include a level sensor in the last compartment for generating volume data; a control valve for controlling the liquid level in the last compartment; and a controller which receives volume data from the level sensor and controls operation of the control valve.

Pressure relief for multiple polyolefin polymerization reactors

A polyolefin manufacturing system and method including polymerizing olefin in a first reactor to form a polyolefin, transferring the polyolefin to a second reactor, polymerizing olefin in the second reactor, and discharging a product polyolefin from the second reactor. The system and method including operating the first reactor with a first reactor pressure relief system and the second reactor with a second reactor pressure relief system, both pressure relief systems to discharge to a flare system, and wherein a relief instrumented system (RIS) is configured to direct at least one process interlock that mitigates an excess reaction scenario as an overpressure relief scenario.

Fenton reactor with gaseous agitation

A Fenton apparatus of the present disclosure includes a reactor vessel, gas injection inlets that allow ejection of aeration coolant perpendicular to axis of the reactor vessel to agitate a reaction composition present in the reactor vessel under vortex conditions, a jacket cooling loop encasing the reactor vessel to allow circulation of a jacket coolant selected from a group consisting of forced air, nitrogen gas, and water, a coil cooling loop coiling around the reactor vessel to allow circulation of a coil coolant selected from a group consisting of forced air, nitrogen gas, water, and carbon dioxide. Multiple programmable solenoid valves are provided to individually control injection of the aeration coolant, the jacket coolant, and the coil coolant. A controller is provided to communicate with a temperature sensor and each programmable solenoid valve.

Methods of Controlling Shutdown of Reactor Systems

Controlling the shutdown of a polyethylene reactor system that includes a secondary compressor, a reactor, a high pressure let down valve (HPLDV), a high-pressure separator, and a high-pressure recycle gas system is provided. After a partial or complete shutdown of secondary compressor, HPLDV opens to a pre-set open position until the reactor pressure reduces to either a pre-set reduced pressure limit or a until the slope of the reactor gas density to reactor pressure exceeds 0.15. The HPLDV controls the pressure to a pressure set point.

Fenton apparatus for safety of industrial exothermic reactions

A Fenton apparatus of the present disclosure includes a reactor vessel, gas injection inlets that allow ejection of aeration coolant perpendicular to axis of the reactor vessel to agitate a reaction composition present in the reactor vessel under vortex conditions, a jacket cooling loop encasing the reactor vessel to allow circulation of a jacket coolant selected from a group consisting of forced air, nitrogen gas, and water, a coil cooling loop coiling around the reactor vessel to allow circulation of a coil coolant selected from a group consisting of forced air, nitrogen gas, water, and carbon dioxide. Multiple programmable solenoid valves are provided to individually control injection of the aeration coolant, the jacket coolant, and the coil coolant. A controller is provided to communicate with a temperature sensor and each programmable solenoid valve.

PERFORMIC ACID PRODUCTION SYSTEMS AND METHODS

Systems for producing performic acid and methods for producing performic acid. The systems may include two or more reactor units, two or more servient programmable logic controllers, a control panel, and a master programmable logic controller. The system may modify the production of performic acid in at least one of the two or more reactor units upon and/or after the occurrence of a disruptive event in order to maintain a desired level of performic acid production and/or a desired level of disinfection.